{"id":1520,"date":"2025-04-24T06:27:33","date_gmt":"2025-04-24T06:27:33","guid":{"rendered":"https:\/\/medpharma12.com\/?p=1520"},"modified":"2025-04-24T06:27:33","modified_gmt":"2025-04-24T06:27:33","slug":"qualitative-analysis-of-unknown-organic-compound-s-for-preliminary-tests","status":"publish","type":"post","link":"https:\/\/medpharma12.com\/index.php\/2025\/04\/24\/qualitative-analysis-of-unknown-organic-compound-s-for-preliminary-tests\/","title":{"rendered":"Qualitative analysis of unknown organic compound\/s for preliminary tests."},"content":{"rendered":"<p><span style=\"color: #333333;\"><strong>EXPERINMENT 02<\/strong><\/span><\/p>\n<p><span style=\"color: #333333;\"><strong>Object<\/strong><\/span><\/p>\n<p><span style=\"color: #000000;\">Qualitative analysis of unknown organic compound\/s for preliminary tests.<\/span><\/p>\n<p><span style=\"color: #333333;\"><strong>Reference<\/strong><\/span><\/p>\n<ol>\n<li><span style=\"color: #000000;\">Vogel Arthere, Elementary practical organic chemistry, 2nd edition, 1966, published by CBS publisher, page No. 61-64.<\/span><\/li>\n<li><span style=\"color: #000000;\">Agarwal O.P., Practical Organic chemistry, published by Krishna educational publisher, Edition 2014, page no. 31-32.<\/span><\/li>\n<\/ol>\n<p><span style=\"color: #000000;\"><strong>Requirement<\/strong><\/span><\/p>\n<p><span style=\"color: #000000;\">Test tube, spatula, different compound, glass-rod etc<\/span><\/p>\n<p><span style=\"color: #000000;\"><strong>Theory<\/strong><\/span><\/p>\n<p><span style=\"color: #000000;\">Preliminary qualitative analysis of an unknown organic compound involves initial tests to determine the compound&#8217;s general properties and the presence of specific elements and functional groups. These tests include physical examination, solubility tests, and flame tests.<\/span><\/p>\n<table>\n<tbody>\n<tr>\n<td width=\"55\"><span style=\"color: #000000;\"><strong>\u00a0<\/strong><\/span><\/td>\n<td width=\"138\"><span style=\"color: #000000;\"><strong>Test<\/strong><\/span><\/td>\n<td width=\"144\"><span style=\"color: #000000;\"><strong>Observation<\/strong><\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\"><strong>Inferences<\/strong><\/span><\/td>\n<\/tr>\n<tr>\n<td rowspan=\"2\" width=\"55\"><span style=\"color: #000000;\"><strong>1<\/strong><\/span><\/td>\n<td rowspan=\"2\" width=\"138\"><span style=\"color: #000000;\"><strong>(a)\u00a0 Nature<\/strong><\/span><\/td>\n<td width=\"144\"><span style=\"color: #000000;\">i)\u00a0\u00a0 Solid<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Carbohydrate, acid, phenol, amine , higher hydrocarbon may be present.<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">ii)\u00a0\u00a0 Liquid<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Alcohol , ketone , aldehyde, ester, phenol, amines may be present.\u00a0<\/span><\/td>\n<\/tr>\n<tr>\n<td rowspan=\"7\" width=\"55\"><span style=\"color: #000000;\"><strong>2<\/strong><\/span><\/td>\n<td rowspan=\"7\" width=\"138\"><span style=\"color: #000000;\"><strong>(b)\u00a0 Colour<\/strong><\/span><\/td>\n<td width=\"144\"><span style=\"color: #000000;\">Yellow -Solid<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">m- Dinitrobenzene, p- Nitro toluene, nitro phenol , nitro aniline<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">Yellow -liquid<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Nitrobenzene.<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">Brown<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">P \u2013 Toluidine , resorcinol.<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">Blackish<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">\u03b1 \u2013 Naphthol<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">Pink<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">\u00df \u2013 Naphthol<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">Buff or reddish<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Aniline, phenol, Aromatic amine.<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">Colourless<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Simple acid , alcohol, ester, ketone aromatic hydrocarbon.<\/span><\/td>\n<\/tr>\n<tr>\n<td rowspan=\"7\" width=\"55\"><span style=\"color: #000000;\"><strong>3<\/strong><\/span><\/td>\n<td rowspan=\"7\" width=\"138\"><span style=\"color: #000000;\"><strong>Odour<\/strong><\/span><\/td>\n<td width=\"144\"><span style=\"color: #000000;\">Carbolic<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Phenol, cresol.<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">Fishy<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Amine<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">Sweet pleasant<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Ester, alcohol and halogen derivatives.<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">Bitter almonds<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Nitrobenzene,Benzaldehyde<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">Moth balls<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Naphthalene<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">No particular\u00a0 smell<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Aromatic acid ,amide, carbohydrate<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\"><strong>\u00a0<\/strong><\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\"><strong>\u00a0<\/strong><\/span><\/td>\n<\/tr>\n<tr>\n<td rowspan=\"3\" width=\"55\"><span style=\"color: #000000;\"><strong>4<\/strong><\/span><\/td>\n<td rowspan=\"3\" width=\"138\"><span style=\"color: #000000;\"><strong>Flame Test<\/strong><\/span><\/td>\n<td width=\"144\"><span style=\"color: #000000;\">Sooty flame<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Aromatic compound or aliphatic compound containing small proportion of hydrogen e.g . CHCI3,CCI4<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">Non sooty flame<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Aliphatic compound<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">Substance chars<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Carbohydrate, sulphanilic acid.<\/span><\/td>\n<\/tr>\n<tr>\n<td rowspan=\"2\" width=\"55\"><span style=\"color: #000000;\"><strong>5<\/strong><\/span><\/td>\n<td rowspan=\"2\" width=\"138\"><span style=\"color: #000000;\"><strong>Test\u00a0 for\u00a0 unsaturation <\/strong><\/span><\/p>\n<p><span style=\"color: #000000;\"><strong>1. KMnO4 test. Substance + 2 ml of water shake well + 2 drops of dilute KMnO4 solution<\/strong><\/span><\/td>\n<td width=\"144\"><span style=\"color: #000000;\">Decolourisation of KMnO4<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Saturated compound.<\/span><\/td>\n<\/tr>\n<tr>\n<td width=\"144\"><span style=\"color: #000000;\">No decolourisation<\/span><\/td>\n<td width=\"301\"><span style=\"color: #000000;\">Unsaturated compound.<\/span><\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<p><span style=\"color: #000000;\"><strong>\u00a0<\/strong><\/span><\/p>\n<p><span style=\"color: #000000;\"><strong>Result: <\/strong>Qualitative analysis of unknown organic compound\/s for preliminary tests was done successfully.<\/span><\/p>\n","protected":false},"excerpt":{"rendered":"<p>EXPERINMENT 02 Object Qualitative analysis of unknown organic compound\/s for preliminary tests. Reference Vogel Arthere, Elementary practical organic chemistry, 2nd edition, 1966, published by CBS publisher, page No. 61-64. Agarwal O.P., Practical Organic chemistry, published by Krishna educational publisher, Edition 2014, page no. 31-32. Requirement Test tube, spatula, different compound, glass-rod etc Theory Preliminary qualitative [&hellip;]<\/p>\n","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"site-sidebar-layout":"default","site-content-layout":"","ast-site-content-layout":"default","site-content-style":"default","site-sidebar-style":"default","ast-global-header-display":"","ast-banner-title-visibility":"","ast-main-header-display":"","ast-hfb-above-header-display":"","ast-hfb-below-header-display":"","ast-hfb-mobile-header-display":"","site-post-title":"","ast-breadcrumbs-content":"","ast-featured-img":"","footer-sml-layout":"","theme-transparent-header-meta":"default","adv-header-id-meta":"","stick-header-meta":"","header-above-stick-meta":"","header-main-stick-meta":"","header-below-stick-meta":"","astra-migrate-meta-layouts":"set","ast-page-background-enabled":"default","ast-page-background-meta":{"desktop":{"background-color":"var(--ast-global-color-4)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"tablet":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"mobile":{"background-color":"","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""}},"ast-content-background-meta":{"desktop":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"tablet":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""},"mobile":{"background-color":"var(--ast-global-color-5)","background-image":"","background-repeat":"repeat","background-position":"center center","background-size":"auto","background-attachment":"scroll","background-type":"","background-media":"","overlay-type":"","overlay-color":"","overlay-opacity":"","overlay-gradient":""}},"footnotes":"","_glsr_average":0,"_glsr_ranking":0,"_glsr_reviews":0},"categories":[1],"tags":[],"_links":{"self":[{"href":"https:\/\/medpharma12.com\/index.php\/wp-json\/wp\/v2\/posts\/1520"}],"collection":[{"href":"https:\/\/medpharma12.com\/index.php\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/medpharma12.com\/index.php\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/medpharma12.com\/index.php\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/medpharma12.com\/index.php\/wp-json\/wp\/v2\/comments?post=1520"}],"version-history":[{"count":1,"href":"https:\/\/medpharma12.com\/index.php\/wp-json\/wp\/v2\/posts\/1520\/revisions"}],"predecessor-version":[{"id":1521,"href":"https:\/\/medpharma12.com\/index.php\/wp-json\/wp\/v2\/posts\/1520\/revisions\/1521"}],"wp:attachment":[{"href":"https:\/\/medpharma12.com\/index.php\/wp-json\/wp\/v2\/media?parent=1520"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/medpharma12.com\/index.php\/wp-json\/wp\/v2\/categories?post=1520"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/medpharma12.com\/index.php\/wp-json\/wp\/v2\/tags?post=1520"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}